| Probe | HCN_0775_sem | HCN_3512_sem |
| Shims | HCN_0775_sem_lk_d20 | HCN_3512_sem_lk_d2o |
| h1pw90 | 7.8us @ 52 | 7.5us @ 51 |
| lshp_ns | 0.74/8.59/10.6 | 0.60/5.18/8.09 |
| lshp | 0.33/2.73/4.92 | 0.30/1.89/2.09 |
| h1sn | 702:1 | 877:1 |
| f19pw90 | 9us @ 52 | — |
| f19sn | 109:1 | — |
| c13pwx | 14.8us @ 60 | 24.7us @ 60 |
| c13gamah2 | 8065 @ 43 | 8065 @ 48 |
| n15pwx | 33us @ 60 | — |
| gzprofile | 32.8 G/cm | 62.8 G/cm |
| gzrecovery | < 1ms | < 1ms |
All shims, probe files and gradient maps saved under /home/vnmr1/vnmrs/ and /vnmr/.
SMS alignment off by about 1/2 cm causing sample move failure. Re-aligned SMS. Ve Re Rt CP1:AT.HAND.GP 2.0 30.4 90.0 CP1:CLEAR.HAND.GP 23.0 0.0 90.0 HAND.GP 16.5 19.9 90.1 CP31:RACK P1 19.5 4.7 76.6 CP31:RACK P2 19.5 4.7 43.7 CP31:RACK P3 19.5 27.2 49.7 CP191:MAGNET 13.4 29.6 259.3 CP191:CLEAR 34.0 0.0 259.3
Repaired various issues with the DD2 400, and Mercury 400. Also, had to figure out how to setup Mercury for Q-Tune because it has a protune accessory. Mercury also had a bad High Band transmitter that had several steps from its attenuator bad.
Customer reported that they could not lock (using 2H) or gradient shim. Looked at 2H RF path and good signal coming out of console to probe. Problem must be on receive side. Swapped the following parts for troubleshooting: 2H Diplexer Lock Preamp 2H RF Relay (verified operation) 2H Filter (bypassed) Believe issue is the Mixer…
Filled three NMR magnets using 100L dewer (filled with only 70L). Magnet Start End Total Oxford 500 34% 100% 66% 72L 40L 32L 10:10 10:35 25 mins Oxford 300 Unknown 100% NA 40L 25L 15L 10:45 10:55 10 mins Bruker 500 80% 100% 20% 25L 0L 25L 11:00 11:15 15 mins
De-Energize Varian Magnex 600 Magnet De-Energized magnet using three supplies set as follows: Supply 1 – Main Supply 2 – RPS / Z0 Supply 3 – Z2 Supply 1 and 2 applied thru the 10-way connector on the neck tube. Supply 3 applied thru the shim stick. Main heater would not open when it was…
De-Energize and Pack De-energized and packed system for shipment to Canada. System was de-energized and warmed up and then packed into Oxford shipping crate (including sides). Four pieces were shipped to IET for final crating and packing. Customer arranged for pickup by a freight carrier. Found the following issued during benchmark; Remote Status box inop…