Settings for dof during pwxcal
| H1 | 13C | 15N | 31P |
|---|---|---|---|
| 300 | -9000 | -9200 | 7000 |
| 400 | -11000 | -12000 | 9000 |
| 500 | -14500 | 0 | 12000 |
| 600 | -17000 | 700 | 14000 |
| 750 | -21000 | 1100 | 17500 |
| 800 | -22600 | 1200 | 18500 |
| J | 151 | 86 | 20 |
The closest thing there is is the np checklist. The one other thing that may give you a clue as to the culprit if the problem is reproducible, is to run debug. You will need to set up mini com. In a terminal window, cd script filename start minicom In the VnmrJ command line, type…
To add the display of Protune during tuning type the following. create(‘showprotunegui’,’string’,’global’) showprotunegui=’y’
Adjusting Mass Flow on a Varian Cryo Platform. Gas Regulator Tuning Procedure (MK1) With the CCC cold and operating at equilibrium (running at least 3 hours), the gas regulator valve should quickly be closed to finger tight and then opened 5 turns. The vernier needle valve on the inlet side of the cold loop should…
Consoles with a PPC may not boot up because the bootfile in /etc/bootptab is VxWorks, and not vxWorksPPC. Change this. Also, change the bootfile in /vnmr/acq/bootptab to vxWorksPPC or a subsequent setacq will overwrite the bootfile name. The PPC should have the bootfile (vxWorksPPC) in nvram, and on boot, the console requests the bootfile. The…
VnmrJ Tips and Tricks
NMR Reference Standards from Millipore Sigma