Settings for dof during pwxcal
| H1 | 13C | 15N | 31P |
|---|---|---|---|
| 300 | -9000 | -9200 | 7000 |
| 400 | -11000 | -12000 | 9000 |
| 500 | -14500 | 0 | 12000 |
| 600 | -17000 | 700 | 14000 |
| 750 | -21000 | 1100 | 17500 |
| 800 | -22600 | 1200 | 18500 |
| J | 151 | 86 | 20 |
VnmrJ Tips and Tricks
SMS Settings TRAY.SIZE=50TRAY.NUMBER=2100 (for 50 samples)TRAY.NUMBER=2050 (for 100 samples) CP31:RACK => 1-50CP32:RACK => 51-100 Typical vertical is 19.2 above rack while training. To format a 720KB floppy +> format a: /T:80 /N:9
NMR Reference Standards from Millipore Sigma
BBOD When VnmrJ starts and the status says “Initializing” or VnmrJ does not start the problem is some inconsistency in the network. VnmrJ adm will start even if VnmrJ does not, but will also come up with the black bar of death “Initializing”. In /etc/hosts, check that the hostname and the IP address are correct….
Calibrate the Mass Flow Meter and Pressure Transducers. 1. Follow the procedures in “Calibration of Mass Flow Meter and Pressure Transducers” 2. Continue with “Adjust the Mass Flow and Ballast Tank Valves,” Adjust the Mass Flow and Ballast Tank Valves Procedure for reduction of vibrations associated with the compressed gas. 1. Remove the housing surrounding the CCC….
Consoles with a PPC may not boot up because the bootfile in /etc/bootptab is VxWorks, and not vxWorksPPC. Change this. Also, change the bootfile in /vnmr/acq/bootptab to vxWorksPPC or a subsequent setacq will overwrite the bootfile name. The PPC should have the bootfile (vxWorksPPC) in nvram, and on boot, the console requests the bootfile. The…